Improving the properties of polymer blends by reactive compounding van der Wal, Douwe Jurjen

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1 University of Groningen Improving the properties of polymer blends by reactive compounding van der Wal, Douwe Jurjen IMPORTANT NOTE: You are advised to consult the publisher's version (publisher's PDF) if you wish to cite from it. Please check the document version below. Document Version Publisher's PDF, also known as Version of record Publication date: 1998 Link to publication in University of Groningen/UMCG research database Citation for published version (APA): van der Wal, D. J. (1998). Improving the properties of polymer blends by reactive compounding Groningen: s.n. Copyright Other than for strictly personal use, it is not permitted to download or to forward/distribute the text or part of it without the consent of the author(s) and/or copyright holder(s), unless the work is under an open content license (like Creative Commons). Take-down policy If you believe that this document breaches copyright please contact us providing details, and we will remove access to the work immediately and investigate your claim. Downloaded from the University of Groningen/UMCG research database (Pure): For technical reasons the number of authors shown on this cover page is limited to 10 maximum. Download date:

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3 Bulk plastics Verreweg de meest gebruikte plastics zijn polyetheen en polypropeen. Deze materialen zijn relatief makkelijk te verwerken en te vormen in een gewenste vorm. Populaire toepassingen zijn verpakkingen, behuizingen van huishoudapparatuur, kinder speelgoed, stoelen, opslagvaten etc. Een belangrijke stroom die voor herverwerking belangrijk is wordt gevormd door verpakkingsmaterialen. Zo worden er enorme hoeveelheden polyetheen en polypropeen verzameld die ingezet zijn in shampoo flessen. Na gebruik worden de flessen verhakt waarna het materiaal opnieuw wordt opgesmolten en in een nieuwe toepassing wordt ingezet. Door de extra verwerking worden de eigenschappen echter minder waardoor de prijs van het materiaal ook lager wordt. Er is vrijwel geen marge op de kiloprijs van deze materialen omdat er enorme hoeveelheden van dit materiaal worden gebruikt. Om de prijs op een acceptabel niveau te kunnen stellen wordt het nodig de eigenschappen van de materialen naar hun oorspronkelijke niveau (of naar een hoger niveau) terug te brengen. Er is dus een methode nodig waarbij de eigenschappen van een plastic worden verbeterd. Om aan alle randvoorwaarden te voldoen is in dit promotiewerk een goedkope methode gezocht waarmee het mogelijk is de eigenschappen van een plastic of een mengsel van plastics te verbeteren. Dit proefschrift. In hoofdstuk 1 wordt de methode beschreven die bedacht is om een chemische verbinding te maken tussen twee plastics als deze door elkaar heen worden gemengd. Hierbij wordt aangenomen dat een chemische hechting tussen beide fases van een mengsel van plastics een noodzakelijke voorwaarde is voor goede eigenschappen van het resulterende product (dit zal een blend worden genoemd). De bolletjes die in figuur 2 te zien zijn moeten hierbij dus via een chemische reactie worden gehecht aan het omliggende materiaal. Een mengsel van polystyreen en polyetheen wordt gebruikt als voorbeeld. De eerste stap in de bedachte methode is om het polyetheen op te zwellen met monomeren. Deze monomeren kunnen na verhitten reageren waarbij ze ook als zijgroep kunnen vast reageren op de polyetheen ketens. Tijdens het proces waarbij het polyetheen wordt gemengd in polystyreen reageert het monomeer zowel met polyetheen als met polystyreen. Hierdoor ontstaat een verbindende keten tussen de beide materialen wat voor de benodigde chemische hechting zorgt tussen de plastics die gemengd worden. De bolletjes in figuur 2 zijn het polyetheen en het omliggende materiaal is polystyreen. Het eerste doel van dit proefschrift is om uit te zoeken of een chemische binding wordt gevormd tussen beide fases van de blend. Het tweede doel om de procescondities hiervoor te optimaliseren. Het derde doel is te bepalen hoe de mechanische eigenschappen van de resulterende blends worden bepaald door de procescondities.

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